Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel
- Autores
- Vaca, Laura Silvia; Quintana, Juan Pablo; Guitar, María Agustina; Vega, Daniel; Brühl, Sonia Patricia; Márquez, Adriana Beatriz
- Año de publicación
- 2019
- Idioma
- inglés
- Tipo de recurso
- artículo
- Estado
- versión publicada
- Descripción
- In this work the influence of pre-treatment cleaning processes in the adhesion of TiN films deposited by the plasma based ion implantation and deposition (PBII&D) process over plasma nitrided AISI 316L stainless steel was investigated, varying the gas composition, the duration of the sputtering process and the temperature in the same deposition chamber. The TiN film morphology was scrutinized with scanning electron microscopy on the surface complemented with focus ion beam for the cross section. The film microstructure was characterized with X ray diffraction. The adhesion of the coatings was studied using the Scratch Test with constant load at different values and the Rockwell C indentation method as well. It was found that only with the sputtering carried out in a H - Ar gas mixing at 300 ºC temperature used as pre-treatment was successful to prepare the nitrided surface for the subsequent TiN deposition by the PBII&D process.
Fil: Vaca, Laura Silvia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina.
Fil: Quintana, Juan Pablo. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina.
Fil: Vega, Daniel. Comisión Nacional de Energía Atómica. Gerencia Investigación y Aplicaciones. Departamento Física de la Materia Condensada; Argentina.
Fil: Brühl, Sonia Patricia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina.
Fil: Márquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina.
Fil:Guitar, María Agustina. Saarland University. Faculty of Natural Sciences and Technology.Material Sciences Department; Germany.
Fil: Márquez, Adriana Beatriz. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina.
Peer Reviewed - Fuente
- Materials Research 22(5), 1-9. (2019)
- Materia
-
PBII&D
TiN films
Adhesion
Duplex treatment - Nivel de accesibilidad
- acceso abierto
- Condiciones de uso
- 2020-12-03T13:41:57Z
- Repositorio
.jpg)
- Institución
- Universidad Tecnológica Nacional
- OAI Identificador
- oai:ria.utn.edu.ar:20.500.12272/4625
Ver los metadatos del registro completo
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Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steelVaca, Laura SilviaQuintana, Juan PabloGuitar, María AgustinaVega, DanielBrühl, Sonia PatriciaMárquez, Adriana BeatrizPBII&DTiN filmsAdhesionDuplex treatmentIn this work the influence of pre-treatment cleaning processes in the adhesion of TiN films deposited by the plasma based ion implantation and deposition (PBII&D) process over plasma nitrided AISI 316L stainless steel was investigated, varying the gas composition, the duration of the sputtering process and the temperature in the same deposition chamber. The TiN film morphology was scrutinized with scanning electron microscopy on the surface complemented with focus ion beam for the cross section. The film microstructure was characterized with X ray diffraction. The adhesion of the coatings was studied using the Scratch Test with constant load at different values and the Rockwell C indentation method as well. It was found that only with the sputtering carried out in a H - Ar gas mixing at 300 ºC temperature used as pre-treatment was successful to prepare the nitrided surface for the subsequent TiN deposition by the PBII&D process.Fil: Vaca, Laura Silvia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina.Fil: Quintana, Juan Pablo. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina.Fil: Vega, Daniel. Comisión Nacional de Energía Atómica. Gerencia Investigación y Aplicaciones. Departamento Física de la Materia Condensada; Argentina.Fil: Brühl, Sonia Patricia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina.Fil: Márquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina.Fil:Guitar, María Agustina. Saarland University. Faculty of Natural Sciences and Technology.Material Sciences Department; Germany.Fil: Márquez, Adriana Beatriz. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina.Peer Reviewed2020-12-03T13:41:57Z2020-12-03T13:41:57Z2019-10-28info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersioninfo:ar-repo/semantics/art??culohttp://purl.org/coar/resource_type/c_6501info:ar-repo/semantics/articuloapplication/pdfapplication/pdfMaterials Research 22(5): 1-9(2019)1980-5373http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000500217&tlng=enhttp://hdl.handle.net/20.500.12272/4625http://dx.doi.org/10.1590/1980-5373-mr-2019-0282Materials Research 22(5), 1-9. (2019)reponame:Repositorio Institucional Abierto (UTN)instname:Universidad Tecnológica Nacionalenginfo:eu-repo/semantics/openAccess2020-12-03T13:41:57Zhttp://creativecommons.org/licenses/by-nc-nd/4.0/Vaca, Laura Silvia ; Quintana, Juan Pablo ; Guitar, María Agustina ; Vega, Daniel ; Brühl, Sonia Patricia ; Márquez, Adriana Beatriz.No comercial con fines académicos2026-09-24T12:45:00Zoai:ria.utn.edu.ar:20.500.12272/4625instacron:UTNInstitucionalhttp://ria.utn.edu.ar/Universidad públicaNo correspondehttp://ria.utn.edu.ar/oaigestionria@rec.utn.edu.ar; fsuarez@rec.utn.edu.arArgentinaNo correspondeNo correspondeNo correspondeopendoar:a2026-09-24 12:45:01.0Repositorio Institucional Abierto (UTN) - Universidad Tecnológica Nacionalfalse |
| dc.title.none.fl_str_mv |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| title |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| spellingShingle |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel Vaca, Laura Silvia PBII&D TiN films Adhesion Duplex treatment |
| title_short |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| title_full |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| title_fullStr |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| title_full_unstemmed |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| title_sort |
Influence of the pre-treatments and process temperature on the adhesion of TiN films deposited by PBII&D over nitrided austenitic stainless steel |
| dc.creator.none.fl_str_mv |
Vaca, Laura Silvia Quintana, Juan Pablo Guitar, María Agustina Vega, Daniel Brühl, Sonia Patricia Márquez, Adriana Beatriz |
| author |
Vaca, Laura Silvia |
| author_facet |
Vaca, Laura Silvia Quintana, Juan Pablo Guitar, María Agustina Vega, Daniel Brühl, Sonia Patricia Márquez, Adriana Beatriz |
| author_role |
author |
| author2 |
Quintana, Juan Pablo Guitar, María Agustina Vega, Daniel Brühl, Sonia Patricia Márquez, Adriana Beatriz |
| author2_role |
author author author author author |
| dc.subject.none.fl_str_mv |
PBII&D TiN films Adhesion Duplex treatment |
| topic |
PBII&D TiN films Adhesion Duplex treatment |
| dc.description.none.fl_txt_mv |
In this work the influence of pre-treatment cleaning processes in the adhesion of TiN films deposited by the plasma based ion implantation and deposition (PBII&D) process over plasma nitrided AISI 316L stainless steel was investigated, varying the gas composition, the duration of the sputtering process and the temperature in the same deposition chamber. The TiN film morphology was scrutinized with scanning electron microscopy on the surface complemented with focus ion beam for the cross section. The film microstructure was characterized with X ray diffraction. The adhesion of the coatings was studied using the Scratch Test with constant load at different values and the Rockwell C indentation method as well. It was found that only with the sputtering carried out in a H - Ar gas mixing at 300 ºC temperature used as pre-treatment was successful to prepare the nitrided surface for the subsequent TiN deposition by the PBII&D process. Fil: Vaca, Laura Silvia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina. Fil: Quintana, Juan Pablo. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Fil: Vega, Daniel. Comisión Nacional de Energía Atómica. Gerencia Investigación y Aplicaciones. Departamento Física de la Materia Condensada; Argentina. Fil: Brühl, Sonia Patricia. Universidad Tecnológica Nacional. Facultad Regional Concepción del Uruguay. Departamento Ingeniería Electromecánica. Grupo de Ingeniería de Superficies; Argentina. Fil: Márquez, Adriana Beatriz. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Fil:Guitar, María Agustina. Saarland University. Faculty of Natural Sciences and Technology.Material Sciences Department; Germany. Fil: Márquez, Adriana Beatriz. Universidad de Buenos Aires. Facultad de Ciencias Exactas y Naturales; Argentina. Peer Reviewed |
| description |
In this work the influence of pre-treatment cleaning processes in the adhesion of TiN films deposited by the plasma based ion implantation and deposition (PBII&D) process over plasma nitrided AISI 316L stainless steel was investigated, varying the gas composition, the duration of the sputtering process and the temperature in the same deposition chamber. The TiN film morphology was scrutinized with scanning electron microscopy on the surface complemented with focus ion beam for the cross section. The film microstructure was characterized with X ray diffraction. The adhesion of the coatings was studied using the Scratch Test with constant load at different values and the Rockwell C indentation method as well. It was found that only with the sputtering carried out in a H - Ar gas mixing at 300 ºC temperature used as pre-treatment was successful to prepare the nitrided surface for the subsequent TiN deposition by the PBII&D process. |
| publishDate |
2019 |
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2019-10-28 2020-12-03T13:41:57Z 2020-12-03T13:41:57Z |
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info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion info:ar-repo/semantics/art??culo http://purl.org/coar/resource_type/c_6501 info:ar-repo/semantics/articulo |
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article |
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publishedVersion |
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Materials Research 22(5): 1-9(2019) 1980-5373 http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000500217&tlng=en http://hdl.handle.net/20.500.12272/4625 http://dx.doi.org/10.1590/1980-5373-mr-2019-0282 |
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Materials Research 22(5): 1-9(2019) 1980-5373 |
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http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14392019000500217&tlng=en http://hdl.handle.net/20.500.12272/4625 http://dx.doi.org/10.1590/1980-5373-mr-2019-0282 |
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eng |
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eng |
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info:eu-repo/semantics/openAccess 2020-12-03T13:41:57Z http://creativecommons.org/licenses/by-nc-nd/4.0/ Vaca, Laura Silvia ; Quintana, Juan Pablo ; Guitar, María Agustina ; Vega, Daniel ; Brühl, Sonia Patricia ; Márquez, Adriana Beatriz. No comercial con fines académicos |
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openAccess |
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2020-12-03T13:41:57Z http://creativecommons.org/licenses/by-nc-nd/4.0/ Vaca, Laura Silvia ; Quintana, Juan Pablo ; Guitar, María Agustina ; Vega, Daniel ; Brühl, Sonia Patricia ; Márquez, Adriana Beatriz. No comercial con fines académicos |
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application/pdf application/pdf |
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